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Synthesis of some pyridoxine and pyridoxal halophosphonates
Croatica Chemica Acta, 69 (1996), 3; 1239-1249. urn:nbn:hr:163:608228
Elshani, Sadik; Butula, Ljubica; Matijević-Sosa, Julija

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Elshani, S., Butula, Lj. i Matijević Sosa, J. (1996). Synthesis of some pyridoxine and pyridoxal halophosphonates. Croatica Chemica Acta, 69. (3), 1239-1249. Preuzeto s https://urn.nsk.hr/urn:nbn:hr:163:608228

Elshani, Sadik, et al. "Synthesis of some pyridoxine and pyridoxal halophosphonates." Croatica Chemica Acta, vol. 69, br. 3, 1996, str. 1239-1249. https://urn.nsk.hr/urn:nbn:hr:163:608228

Elshani, Sadik, Ljubica Butula i Julija Matijević Sosa. "Synthesis of some pyridoxine and pyridoxal halophosphonates." Croatica Chemica Acta 69, br. 3 (1996): 1239-1249. https://urn.nsk.hr/urn:nbn:hr:163:608228

Elshani, S., Butula, Lj. i Matijević Sosa, J. (1996) 'Synthesis of some pyridoxine and pyridoxal halophosphonates', Croatica Chemica Acta, 69(3), str. 1239-1249. Preuzeto s: https://urn.nsk.hr/urn:nbn:hr:163:608228 (Datum pristupa: 20.04.2024.)

Elshani S, Butula Lj, Matijević Sosa J. Synthesis of some pyridoxine and pyridoxal halophosphonates. Croatica Chemica Acta [Internet]. 1996. [pristupljeno 20.04.2024.];69(3):1239-1249. Dostupno na: https://urn.nsk.hr/urn:nbn:hr:163:608228

S. Elshani, Lj. Butula i J. Matijević Sosa, "Synthesis of some pyridoxine and pyridoxal halophosphonates", Croatica Chemica Acta, vol. 69, br. 3, str. 1239-1249, 1996. [Online]. Dostupno na: https://urn.nsk.hr/urn:nbn:hr:163:608228. [Citirano: 20.04.2024.]

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Podaci o radu
Naslov (engleski)Synthesis of some pyridoxine and pyridoxal halophosphonates
AutorSadik Elshani
AutorLjubica Butula
MBZ: 6383
AutorJulija Matijević-Sosa
Autorova ustanovaSveučilište u Zagrebu
Farmaceutsko-biokemijski fakultet
(Zavod za biokemiju i molekularnu biologiju)
Znanstveno / umjetničko
područje, polje i grana		BIOMEDICINA I ZDRAVSTVO
Farmacija
Medicinska biokemija
Sažetak (engleski)
A new series of pyridoxine and pyridoxal chloro and fluorophosphonates have been synthesized. Partially protected pyridoxine 1, 2 or pyridoxal 4 reacted with methyl phosphonic dichloride in the presence of triethylamine at -10 °C. Thus, the following chlorophosphonate derivatives were obtained: 3,4'-0-isopropylidenepyridoxine-5'-0- methylchlorophosphonate (5), 4',5'-0-isobutylidenepyridoxine-3-0- methylchlorophosphonate (6), and monoethylacetalpyridoxal-3-0- methylchlorophosphonate (7). Similarly, from adequate starting compounds 1,3 and unprotected pyridoxal (PL) in the reaction with methyl phosphonic difluoride and triethylamine, near O"C, the corresponding 3-0 or 5'-0-methylfluorophosphonateswere obtained; 3,4'-0 isopropylidenepyridoxine-5'-0-methylfluorophosphonate(8), 4-metoxymethylpyridoxine- 5'-0-methylfluorophosphonate (9) and pyridoxal- 5'-0-methylfluorophosphonate (10).
Jezikengleski
Vrsta publikacijeZnanstveni rad - Izvorni znanstveni rad
Status objaveObjavljen
Vrsta recenzijeRecenziran - međunarodna recenzija
Verzija publikacijeObjavljena verzija rada (izdavačev PDF)
Naslov časopisaCroatica Chemica Acta
Brojčani podacivol. 69, br. 3, str. 1239-1249
p-ISSN0011-1643
e-ISSN1334-417X
URN:NBNurn:nbn:hr:163:608228
Datum objave publikacije1996
URL dokumentahttps://hrcak.srce.hr/177142
Vrsta resursaTekst
Prava pristupaOtvoreni pristup
Uvjeti korištenjaIkona licence Zaštićeno autorskim pravom.
Datum i vrijeme pohrane2020-04-29 14:29:56